Local Enrichment of Active Element Y in Y-modified PVD Films on Mild Steel Substrate

By means of EPMA,SIMS and XTEM tech-niques,the element distribution at the transitionzone of Y-modified ion plated titanium andtitanium nitride film on A3 steel substrate and thevariation of the element content on the surface ofthe evaporation source before and after service werestudied in detail.A mode was proposed in terms ofpreferential evaporation and micro-tunnel trans-portation of Y at the interface of film/substrate.     

Activity of NiO in (Ni,Mg)O Solid Solutions

Disagreement exists in the literature concerting the activity of NiO in (Ni,Mg)O solid solutions. Ideal behavior, as well as strong positive deviations and strong negative deviations from ideality, has been reported. In the present study, the activity of NiO was determined by electromotive force measurements using the solid-state cell Pt/Ni-NiO/0.92ZrO₂-0.08Y₂O₃/Ni-(Ni,Mg)O/Pt. The compositions studied had NiO mole fractions of 0.1,0.3,0.5,0.7, and 0.9. In agreement with theoretical expectations, the solid solutions exhibited ideal behavior at 882° and 982°C. Possible reasons for the conflicting results in the literature arc presented.     

Energy release rates of crack kinking by boundary condition sensitivity analysis

The energy release rate, which is the total derivative of the energy with respect to crack length, is recognized as corresponding to the shape sensitivity analysis with the crack length change represented by the tangential component of design velocity. In this paper the sensitivity formula recently developed for a changing boundary condition has been further extended to cover crack kinking under mixed mode loading. Due to difficulty in defining the velocity field at the corner, the energy release rate at the onset of crack kinking is obtained by extrapolating the energy release rates for finite length kinked cracks. A rectangular plate with a single edge slant crack under uniform tension is taken as a numerical example. The multi-region technique in the numerical implementation of the boundary integral equation is adopted to consider the asymmetry of the problem. Excellent accuracy is observed as compared with reference analytic solutions.     

正义峡坝址基础岩体灌浆质量检测

采用声波测井、地震CT等综合物探方法 ,对正义峡水库坝址基础岩体固结灌浆质量进行检测 ,基本查明了坝基岩体固结灌浆后的质量状况 ,取得了良好的应用效果     

碳纤维表面处理对铝电解用硼化钛阴极涂层性能的影响

硼化钛阴极涂层是铝电解用可润湿性阴极材料中的一种，具有优良的抗钠渗透性和对铝液润湿性，可以有效地延长铝电解槽寿命。碳纤维是硼化钛涂层材料的增强剂之一．对硼化钛阴极涂层的性能影响很大。本文研究了不同工艺的液相碳纤维表面氧化处理法对硼化钛阴极涂层抗拉强度和粘接强度的影响。采用PTIR检测碳纤维处理后表面含氧基团的变化，寻找影响硼化钛阴极涂层性能的原因，从而达到最有效地提高TiB2阴极涂层抗拉强度和粘接强度的目的。结果表明，采用工艺(1)(10％HNO3，80℃、恒温5min．超声波、5min)对碳纤维进行表面处理最合理，处理后碳纤维表面含氧基团的含量最高．用其制备硼化钛阴极涂层的抗拉强度、粘接强度最大。     

基于ObjectAgent的小卫星星务系统研究与仿真

针对小卫星自主管理与自主决策的要求,简单介绍了多Agent技术和ObjectAgent开发环境,并以某小卫星为例,研究并设计了基于ObjectAgent的小卫星星务系统,给出了所涉及的Agent的自主决策、任务调度、信息交互等一系列问题的解决方案,最后,利用多台PC机组网进行了仿真,达到了预期的实验效果。     

硅中硼离子注入校准样品的研制

本文主要介绍了硅中硼离子注入校准样品的制备与研究。分别用三台SIMS仪器对样品进行了深度剖析与比对,并对用作校准目的的样品主要参数进行了定值。     

超声波处理石油污水的实验研究

考察了在不同空化状态下超声波对石油污水化学耗氧量(COD)的降低作用。探讨了时间、功率、pH值及温度对石油污水化学耗氧量降低作用的影响。结果表明，石油污水化学耗氧量的降低率随着时间增大而增大，随着温度、pH值的增加而减小，随着功率的增加，先增加，然后再减小。     

微波萃取在食品化学中的应用

介绍了微波萃取技术在食品化学中的应用。其实质是用微波对萃取溶剂及物料加热，使溶剂的渗透率和扩散率大大提高，因此对食品营养成分或风味物质可以有铲地萃取分离。